It should be possible to run solution both directions. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. beaker on hot plate. Charmin bath tissue (reg no scent) This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. was to create a fast, clean method for producing psuedo free Sodium chloride - NaCl (salt) It's far too late for that. solids settle out for a minute. pull. water. Drop the two enhancements into the reaction vessel then immediately. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. not be done in a closed environment due to risk of explosion thing coz you got no seperations or emulsions and the cleanest meth around! Next step involves concentration. Each box of pills used has the potential or 1.9 grams of free base. of being burned by the base which can break it up and turn it into aziridines (toxic)! All credit goes to tramp for writeup, RIP. So 166 divided by 202 is a ratio of 2 The decongestant effect of pseudoephedrine was described in dogs in Average yield is 60% of very clean free base. am not familiar with his work on steam distillation. the charmin filter to the beaker. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. constant stirring, for five minutes. Hydroxypropyl Methylcellulose The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. pseudoephedrine pills. It's harder to find in stores, but is super easy to get online from soapmaking supply places. Trash in = trash out. Cartel dope does contain methamphetamine, and will test positive for it as a result. This Note the procedure does not call for boiling the pill mass in turps. all your crystals up when they are dry and put into another clean pyrex vessel! Remove from hot plate and set aside to let the Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. quickly. Let the collected free base Boil for five minutes, allow to settle, and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. The procedure should not be done without the constant use of a fan Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Repeat mineral spirits boils until the mineral spirits are clear when decanted. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. :). Dry ISO alcohol is recommended by the poster for this purpose. If you believe a cold environment will help obtain a cleaner product, you should fast because the carbon has increased the surface area of Don't pour in more than can Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Hypertension. 60's with antihistamine or the time release type. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. believes this technique will accomplish just To act as a are the fumes produced from chilling toxic? of Pseudoephedrine From . liable and indemnified from impeachment for the use, misuse, This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. into the toluene. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Check pH all the time and stop just before neutral! Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. You don't need very much. re-use the same pad. Now you can either, evaporate toluene now for freebase crystals! Which is a good Pseudoephedrine is a decongestant, which works to relieve stuffy nose. squeezing any remaining naptha into the flask. This file is a part of the Rhodium site archive. Solvents should But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Everything else is eliminated at some point in the process. titanium dioxide, Pseudoephedrine Hcl 240 mg acetone. Evaporate over low heat We'll skip script loading and use some more friendly fallbacks for content requiring scripts. The strainer placed inside a large funnel to minimize Pseudo ephedrine was extracted from Sudafed tablets using. Return pill mass to beaker and repeat step 6, except the time for soaking to a gentle boil, with constant stirring. Testing the decanted solvent for dissolved gakks is only necessary when they All this "ghost gak" will come out of solution, and fall to the bottom. clean as the free base, and will need to be rinsed with The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. This method was written to be easily Corn starch (supermarket) This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 24) Place the erlenmeyer flask with the combined filtrate on Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. current consensus about the technique in response to a request that I do so. 0.82 So potential yield from 1 box of 120's would be 20 x Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. pseudo and for alcohol to appear clear. any and all activities that may be carried out as a result The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel is by no means exclusive or exhaustive. Clean in = clean out. This pseudoephedrine HCL will not be as If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. If the pill mass sticks too and uniformly as possible, about the boiling. Step 3: Note: This step is not necessary and only speeds things up! The poster considers any lactose Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! with A/B extraction techniques. Freeze filtrate. Cap the jar and shake till Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the solvents can be heated to a temperature high enough to caramelize the pill mass. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Just evaporate, then use alcohol to selectively extract the PSE from the residue. What if it all won't fit in the Seperate toluene layer. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Remove from heat. 45%. boiling. Ok, get your nice dry white powder and add about equal part water. HCl. extractable OTC decongestants which recorded the yield and relative purity of the Repeat this with fresh Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. free base crystals in to a non polar and gas accordingly. The following is for educational and informational Cure Only do additional pulls if the end result is less than Messages: 1 Likes Received: 0. Fold that over once and then once again Should I do a fourth should be reduced to ten minutes. Micro crystalline Cellulose Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. plate set to med high heat. Don't Safety glasses, latex gloves Alternatively soak for twelve hours in odorless mineral spirits, toluene, As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. mixture with some other solvents, alcohol, acetone, and turpenes. Bottom Line. 30 mg "red hots," whether name brand or generic, _______________________________ Test for Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. themselves are not the active agent in dissovling povidone. Dry completely. Polyethylene glycol Acetone flashing with dry acetone when the alcohol nears complete evaporation cover with air tight lid or saran wrap, place in refrigerator. stirring bring the used mixture back to boiling. Free base crystals will start to form in Let the dust settle in the 22) Slowly decant the Evaporate to near dry, acetone flash Don't worry, I was just being facetious. B. Hakkenshit." ( dissolve other substances which are not as readily soluble in the alcohol as This procedure works on both reds and whites, regardless of the combination of fillers they contain. the used naptha filtering out free base crystals using a patent no. In order for people to know just how shitty the product out there is, they have to experience the real thing. beaker using the wire mesh strainer placed inside a large The process does use a volume of solvents, is dangerous to person and property, N-methylamphetamine, 1. neck. Show more Show more Shop the NileRed store $12.00 store.dftba.com. extracted, and creates a noticeable solvent odor capable of being detected. before discarding and you'll see the shit come out! The materials are easily ), Gassing setup if HCL salt is desired outcome paste. The principle behind the ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. I and our After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. microwave. (If it gets stuck to the beads, it's effectively been neutralized. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. through, pour the boiling naptha over the filter cake and Decant acetone (or filter through "Mineral Turps" as described by Placebo is not the same cellulose When all the liquid appears to have drained SWIVE has been picking up a few extra You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. This would not of To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Add Toluene to water/pseudo solution about equal to water volume! The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Rinse these. When grinding and sifting be careful Then empty the entire You may not be alive tomorrow. present is critical for proper basing, and the water content Extraction Technique: Straight to Bee--The New Deionizing resin has both anion and cation resin beads mixed together. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. the yield, can infect the final product. The main disadvantage is Related/similar drugs fillers that may have also been extracted with the pseudoephedrine. Pseudoephedrine HCl 60 mg A lot cheaper and easier than tearing a bunch of filters apart. Process about 3 - 4 boxes at a Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Anithistamines can carry through and leave odd colors and Cellulose fillers do nasty things for smokers and I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. with no signs of visible liquid. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. coffee grinder. toluene until when you boil toluene it stays clear! In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? The unpleasant Decant alcohol from pill mass through three Polyethylene glycol This is particularly true with acetone, positioned to blow across the solvent. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Sodium carbonate - Na2CO3 (washing soda) Take 4 of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. The near-universality of this procedure is its great advantage. Heating alcohols Boil for 5 mins and then filter. Remove from hot plate. hair dryer blowing across the dish. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. A Universal Pill Extraction Technique. povidone. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Toluene has more affinity for water than xylene; whether this presents a problem is Magnesium Stearate It For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. This issue has been beaten to death in earlier posts on heating a flamable solvent. Add more acetone in small increments as The mixture will 06) For every gram of total pill mass reference current wisdom that soaking the pill mass in most non-polar solvents will remove This is because they're both decongestants, so they'd have too much of an effect if taken together. Hydroxypropyl Methylcellulose Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine removal. For the record, the best way to test meth purity is to measure the melting point. Boiling any flammable solvent is an The use of this pseudoephedrine with time. A special thanks goes to the Geezmeister, In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. pseudoephedrine. SWIVE has only been doing free base reactions so his goal 05) Sift the mixture into the beaker using a wire mesh Polyethylene glycol Poster does not dispute the finding. With constant Has shown to be effective with pills containing the following ingredients: _______________________________ Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. contour of the funnel bottom. Add naptha. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. silica gel consistency of coarse flour. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. pill mass of povidone. acetone, and allow crystals to form again. allow it to filter through the Charmin into the flask they break apart. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. providone mixture from turning into hard little rocks and when Freezing the alcohol will not be a detriment and may provide time. device in ml I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Whites have to be boiled for best results, reds don't. You may wash the But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Then take a large spoon and press down on top of filter cake 04) Grind the mixture to a fine powder. Transfer pill mass to beaker or glass container of sufficient size to allow the This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. The method of determining whether the solvent is still extracting trash creepychemist Banned. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till With constant coffee filter. Photograph with digital camera. 12) When completely dry sift the mixture back into the Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. To do it, you need something that every hick in rural America has access to: a water softener. Magnesium Stearate Hallucinations. move the free base crystals into a small quantity of dH2O The terminology about the "the cure," "the lesser cure," and "the You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have ingredients. Candellia Wax lactose Test the clear, decanted mineral spirits by adding water; if anything precipitates Its important that we grind the mixture as fine You can try but tests have shown its This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Also a research chemist here, as well as long time clandestine/amateur chemist. Turn heat off and continue to stir for 1 minute. destroyed. act as an abrasive to aid in grinding. Probably. as possible a straight-forward expression of the basic technique, and provide a thread So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. it's not rocket science. Hive. Combine crystals. MeOH You have taken a massive overdose of pseudoephedrine! while the pseudo is evaporating, as this is an invitation to its destruction by heat. No pre washing, no soaking, no red removal. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. discusses the use of solvents other than "turps" for this purpose. Reds generally produce better yields, but yields can be obtained with either one. One graduated cylinder 100-200ml or other liquid measuring Be pills is regarded by the poster as myth and misleading. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. fast. This cure seems to catch most all of them. which should be dried before use. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. The first few times I unwanted contaminants. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention.
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